पोटेशियम ज्वाला परीक्षण
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बैंगनी/नीलम ज्वाला से पोटेशियम की पहचान
उद्देश्य
पोटेशियम आयनों द्वारा उत्पन्न बैंगनी/नीलम ज्वाला रंग का अवलोकन करें, और सोडियम संदूषण से इसे अलग करने के लिए कोबाल्ट नीले कांच का उपयोग करना सीखें।
पृष्ठभूमि
Potassium produces a pale lilac or violet flame when heated. The emission occurs at 766.5 nm and 769.9 nm (near-infrared/deep red doublet). Because the flame is quite faint and easily overwhelmed by sodium's intense yellow, cobalt blue glass is used as a filter to block sodium emission and reveal potassium's true color.
सुरक्षा चेतावनियाँ
- Wear safety goggles at all times
- Keep hair tied back near open flames
- Handle HCl with care
आवश्यक PPE
सामग्री
-
Potassium chloride (KCl) (1 g)
-
Hydrochloric acid (HCl) (10 mL)1M concentration
-
Cobalt blue glass (1 piece)For filtering sodium light
उपकरण
प्रक्रिया
Clean the nichrome wire thoroughly by dipping in HCl and heating.
Place potassium chloride on the watch glass and collect a sample on the clean wire.
Hold the sample in the Bunsen burner flame. Observe with the naked eye first.
Now observe the flame through cobalt blue glass to filter out any sodium contamination.
Record the difference in appearance with and without the cobalt blue glass filter.
अपेक्षित परिणाम
Without the filter, you may see a faint lilac color possibly masked by yellow from sodium impurities. Through the cobalt blue glass, a clear violet/lilac flame should be visible as the glass absorbs the yellow sodium emission.
सफाई
Clean the wire loop with HCl. Return cobalt blue glass to storage.
विवरण
- श्रेणी
- Flame Tests
- कठिनाई
- Beginner (Middle School)
- अवधि
- 20 मिनट
- अनुमानित लागत
- $6.00
- चरण
- 5
- सामग्री
- 3