Cristallisation Fractionnée du Sel et du Sable
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Séparation d'un mélange par différences de solubilité
Objectif
Séparer un mélange de sel et de sable par cristallisation fractionnée, démontrant la dissolution, la filtration et la cristallisation par évaporation.
Contexte
This classic separation technique exploits the fact that salt dissolves in water while sand does not. The mixture is dissolved in hot water, filtered to remove sand, and then the salt is recovered by evaporation. This is fundamentally how salt has been harvested from seawater for millennia.
Avertissements de sécurité
- Handle hot evaporating dish with tongs
- Do not heat to dryness too rapidly — spattering risk
EPI requis
Matériaux
-
Salt-sand mixture (10 g)Pre-mixed approximately 50:50
-
Distilled water (100 mL)
Équipement
Procédure
Weigh 10 g of the salt-sand mixture and record the mass.
Add the mixture to 100 mL of warm water in the beaker. Stir for 5 minutes to dissolve all the salt.
Filter the mixture through filter paper. The sand remains on the filter; the salt solution passes through.
Rinse the sand on the filter with a small amount of distilled water. Dry the sand and weigh it.
Pour the filtrate into the evaporating dish. Heat gently on the hot plate to evaporate the water.
Once dry, weigh the recovered salt. Calculate the percentage of each component.
Compare the total recovered mass with the initial mass. Calculate percent recovery.
Résultats attendus
The total mass of recovered salt + sand should be close to the original 10 g (typically 90-98% recovery). Some loss occurs during transfer and on filter paper. The separated components should be visually distinct.
Nettoyage
Salt solution can go down the drain. Sand can go in the trash. Rinse all glassware.
Détails
- Catégorie
- Crystallization
- Difficulté
- Beginner (Middle School)
- Durée
- 35 min
- Coût estimé
- $3,00
- Étapes
- 7
- Matériaux
- 2