塩と砂の分別結晶化
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溶解度の差を利用して混合物を分離する
目的
塩と砂の混合物を分別結晶化で分離し、溶解・ろ過・蒸発結晶化を実証する。
背景
This classic separation technique exploits the fact that salt dissolves in water while sand does not. The mixture is dissolved in hot water, filtered to remove sand, and then the salt is recovered by evaporation. This is fundamentally how salt has been harvested from seawater for millennia.
安全上の警告
- Handle hot evaporating dish with tongs
- Do not heat to dryness too rapidly — spattering risk
必要なPPE
材料
-
Salt-sand mixture (10 g)Pre-mixed approximately 50:50
-
Distilled water (100 mL)
器具
手順
Weigh 10 g of the salt-sand mixture and record the mass.
Add the mixture to 100 mL of warm water in the beaker. Stir for 5 minutes to dissolve all the salt.
Filter the mixture through filter paper. The sand remains on the filter; the salt solution passes through.
Rinse the sand on the filter with a small amount of distilled water. Dry the sand and weigh it.
Pour the filtrate into the evaporating dish. Heat gently on the hot plate to evaporate the water.
Once dry, weigh the recovered salt. Calculate the percentage of each component.
Compare the total recovered mass with the initial mass. Calculate percent recovery.
予想される結果
The total mass of recovered salt + sand should be close to the original 10 g (typically 90-98% recovery). Some loss occurs during transfer and on filter paper. The separated components should be visually distinct.
後片付け
Salt solution can go down the drain. Sand can go in the trash. Rinse all glassware.
詳細
- カテゴリ
- Crystallization
- 難易度
- Beginner (Middle School)
- 所要時間
- 35 分
- 推定費用
- $3.00
- ステップ数
- 7
- 材料
- 2