硫酸銅結晶の育成
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緩慢な蒸発で大きな青色結晶を生成する
目的
緩慢蒸発法を用いて大きく形の整った硫酸銅五水和物の結晶を育成し、過飽和と結晶格子形成を実証する。
背景
Copper sulfate pentahydrate (CuSO₄·5H₂O) forms beautiful blue triclinic crystals. By preparing a saturated solution and allowing it to evaporate slowly over several days, large single crystals can be grown. The process demonstrates concepts of solubility, supersaturation, and crystal nucleation.
安全上の警告
- Copper sulfate is toxic if ingested
- Wear gloves when handling the solution
- Wash hands thoroughly after the experiment
- Do not dispose of copper sulfate down the drain
必要なPPE
材料
-
Copper(II) sulfate pentahydrate (50 g)Blue crystals
-
Distilled water (200 mL)Hot
-
Thread or fishing line (30 cm)For seed crystal
-
Pencil or stick (1)To suspend seed crystal
器具
手順
Heat 200 mL of distilled water to 60-70°C. Add copper sulfate gradually while stirring until no more dissolves (saturated solution).
Filter the hot saturated solution through filter paper to remove any undissolved particles.
Pour a small amount into a petri dish and allow it to cool. Select the best small crystal as a seed crystal after 24 hours.
Tie the seed crystal to a thread and suspend it from a pencil placed across the top of the beaker of saturated solution.
Cover the beaker loosely with filter paper to allow slow evaporation. Place in a vibration-free location.
Check daily for crystal growth. Remove any small crystals that form on the thread or beaker walls.
予想される結果
After 1-2 weeks, the seed crystal should grow into a large blue crystal (1-3 cm) with well-defined facets. The crystal has a triclinic shape with distinct flat faces. Faster evaporation produces many small crystals; slower produces fewer, larger ones.
後片付け
Collect excess copper sulfate solution and solid for reuse or proper disposal in heavy metal waste. Do not pour down the drain.
詳細
- カテゴリ
- Crystallization
- 難易度
- Beginner (Middle School)
- 所要時間
- 30 分
- 推定費用
- $8.00
- ステップ数
- 6
- 材料
- 4