Бариевый пламенный тест
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Определение бария по желтовато-зелёному пламени
Цель
Наблюдать бледно-желтовато-зелёное пламя ионов бария и понять, почему соединения бария требуют особых мер безопасности.
Предпосылки
Barium compounds produce a pale yellow-green (apple-green) flame when heated. The emission is primarily from BaCl molecules formed in the flame rather than from atomic barium. Barium compounds are toxic and require careful handling, but the flame test itself uses small quantities safely.
Предупреждения по безопасности
- Barium chloride is toxic if ingested
- Wear nitrile gloves when handling barium compounds
- Wear safety goggles at all times
- Wash hands thoroughly after the experiment
- Do not eat or drink in the lab
Требуемые СИЗ
Материалы
-
Barium chloride (BaCl₂) (0.5 g)Toxic — handle with care
-
Hydrochloric acid (HCl) (10 mL)1M concentration
-
Distilled water (50 mL)For cleaning
Оборудование
Процедура
Put on nitrile gloves before handling barium chloride.
Clean the nichrome wire by dipping in HCl and heating until no color appears.
Place a small amount of barium chloride on the watch glass.
Dip the clean wire into HCl, then into the barium chloride sample.
Hold the wire in the Bunsen burner flame and observe the pale yellow-green color.
Record the color and compare with copper (blue-green) if previously tested.
Ожидаемые результаты
A pale yellow-green (apple-green) flame should appear. The color is less vivid than copper's blue-green and has a distinctly yellowish tint. It may be difficult to see in a well-lit room.
Уборка
Clean the wire with HCl. Dispose of barium waste in designated heavy metal waste container. Remove gloves carefully and wash hands thoroughly.
Детали
- Категория
- Flame Tests
- Сложность
- Intermediate (High School)
- Продолжительность
- 20 мин
- Прим. стоимость
- $12,00
- Шаги
- 6
- Материалы
- 3