Кальциевый пламенный тест
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Определение кальция по оранжево-красному пламени
Цель
Наблюдать кирпично-красное или оранжево-красное пламя ионов кальция — элемента, содержащегося в известняке, мраморе и костях.
Предпосылки
Calcium produces a distinctive brick-red to orange-red flame color. The emission results from electronic transitions in calcium atoms excited by the flame energy. Calcium is one of the most abundant elements in the Earth's crust and its flame test is a useful diagnostic tool in mineral identification.
Предупреждения по безопасности
- Wear safety goggles at all times
- Keep hair tied back near open flames
- Handle HCl with care
Требуемые СИЗ
Материалы
-
Calcium chloride (CaCl₂) (1 g)Common road de-icer
-
Hydrochloric acid (HCl) (10 mL)1M concentration
-
Distilled water (50 mL)For cleaning
Оборудование
Процедура
Clean the nichrome wire by dipping in HCl and heating until no color appears.
Place calcium chloride on the watch glass and collect a sample on the clean wire.
Hold the wire in the Bunsen burner flame and observe the flame color.
Record the brick-red to orange-red color and note how it differs from strontium and lithium.
Ожидаемые результаты
A brick-red to orange-red flame should appear. The color is less vivid than strontium's scarlet and more orange than lithium's crimson. Calcium's flame is moderate in intensity.
Уборка
Clean the wire with HCl. Dispose of chemicals per lab protocol.
Детали
- Категория
- Flame Tests
- Сложность
- Beginner (Middle School)
- Продолжительность
- 15 мин
- Прим. стоимость
- $5,00
- Шаги
- 4
- Материалы
- 3