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황록색 불꽃으로 바륨 확인하기
목표
바륨 이온이 나타내는 연한 황록색 불꽃을 관찰하고, 바륨 화합물에 추가적인 안전 주의가 필요한 이유를 이해한다.
배경
Barium compounds produce a pale yellow-green (apple-green) flame when heated. The emission is primarily from BaCl molecules formed in the flame rather than from atomic barium. Barium compounds are toxic and require careful handling, but the flame test itself uses small quantities safely.
안전 경고
- Barium chloride is toxic if ingested
- Wear nitrile gloves when handling barium compounds
- Wear safety goggles at all times
- Wash hands thoroughly after the experiment
- Do not eat or drink in the lab
필수 개인 보호 장비
재료
-
Barium chloride (BaCl₂) (0.5 g)Toxic — handle with care
-
Hydrochloric acid (HCl) (10 mL)1M concentration
-
Distilled water (50 mL)For cleaning
장비
실험 절차
Put on nitrile gloves before handling barium chloride.
Clean the nichrome wire by dipping in HCl and heating until no color appears.
Place a small amount of barium chloride on the watch glass.
Dip the clean wire into HCl, then into the barium chloride sample.
Hold the wire in the Bunsen burner flame and observe the pale yellow-green color.
Record the color and compare with copper (blue-green) if previously tested.
예상 결과
A pale yellow-green (apple-green) flame should appear. The color is less vivid than copper's blue-green and has a distinctly yellowish tint. It may be difficult to see in a well-lit room.
정리
Clean the wire with HCl. Dispose of barium waste in designated heavy metal waste container. Remove gloves carefully and wash hands thoroughly.
세부 정보
- 카테고리
- Flame Tests
- 난이도
- Intermediate (High School)
- 소요 시간
- 20 분
- 예상 비용
- $12.00
- 단계
- 6
- 재료
- 3